X-ray scattering techniques for determining the susceptibility of oilfield equipment metal to destruction under load

UDK: 622.276.5.05:543.424
DOI: 10.24887/0028-2448-2024-11-131-134
Key words: corrosion failure, oilfield equipment, microstructure, X-ray phase analysis, anisotropy of strength properties, residual macrostresses
Authors: A.V. Malinin (RN-BashNIPIneft LLC, RF, Ufa); V.D. Sitdikov (RN-BashNIPIneft LLC, RF, Ufa)

The article presents the recent achievements of RN-BashNIPIneft LLC Institute in the development and application of X-ray scattering techniques to solve practical problems related to the determination of metal of oilfield equipment to corrosion damage, flowing under load. To solve these problems, the authors propose to adapt X-ray scattering techniques to the study of steels widely used to manufacture various products for the oil industry. In particular, the technique of X-ray phase analysis has been adapted to determine the type of structural components of steels (austenite, martensite, tempered martensite, bainite, perlite, ferrite) and assess their quantitative ratio in products. As a result, it became possible to establish possible violations of the heat treatment regimes of metal during the formation of a specific structure in steel blanks for the manufacture of oilfield equipment. By analyzing the crystallographic textures of the metal of the product, the predominant grain orientations of various structural components of steels were established, which enabled to identify various types of deformation treatment used in the molding of the final product. It is demonstrated that the analysis of the preferential orientations of steel grains provides important assistance in determining the anisotropy of the strength properties of the metal of oilfield equipment. This information allows one to evaluate the resulting strength in products of complex shape and can be useful in their design.

References

1. Tkacheva V.E., Valekzhanin I.V., Kshnyakin D.V. et al., Serovodorod (H2S): lokal’nye i korrozionno-mekhanicheskie razrusheniya v neftedobyche (Hydrogen sulfide (H2S): local and corrosion-mechanical destruction in oil production), Ufa: Publ. of RN-BashNIPIneft, 2024, 240 p.

2. Nosov V.V., Presnyakov A.Yu., Badamshin A.G. et al., Organochlorine compounds in oil: problems and solutions (In Russ.), Neftyanoe khozyaystvo = Oil Industry, 2021, no. 4, pp. 110–113, DOI: https://doi.org/10.24887/0028-2448-2021-4-110-113

3. Valekzhanin I.V., Voloshin A.I., Development and testing of a module for calculating the parameters of scale inhibitors squeeze treatment (In Russ.), Problemy sbora, podgotovki i transporta nefti i nefteproduktov, 2024, no. 3(149), pp. 43–53, DOI: https://doi.org/10.17122/ntj-oil-2024-3-43-53

4. Gulyaev A.P., Gulyaev A.A., Metallovedenie (Metal science), Moscow: Metallurgiya Publ., 2012, 648 p.

5. Sitdikov V.D., Nikolaev A.A., Ivanov G.V. et al., Microstructure and crystallographic structure of ferritic steel subjected to stress-corrosion cracking, Letters on Materials, 2022, V. 12, no. 1 (45), pp. 65–70, DOI: https://doi.org/10.22226/2410-3535-2022-1-65-70

6. Malinin A.V., Sitdikov, V.D., Kurilov A.A. ,Special features of structural and phase transformations in bainitic steel, Metal Science and Heat Treatment, 2023,

V. 65 (5–6), pp. 265–271, DOI: https://doi.org/10.1007/s11041-023-00924-z

7. Malinin A.V., Sitdikov V.D., Tkacheva V.E. et al., Characteristic properties of the microstructure and microtexture of medium-carbon steel subjected to sulfide stress cracking (In Russ.), Frontier Materials & Technologies, 2023, no. 1, pp. 33–44, DOI: https://doi.org/10.18323/2782-4039-2023-1-33-44

8. Sitdikov V.D., Islamgaliev R.K., Nikitina M.A. et al., Analysis of precipitates in ultrafine-grained metallic materials, Philosophical Magazine, 2019, V. 99, no. 1, pp. 73–91, DOI: https://doi.org/10.1080/14786435.2018.1529443


Attention!
To buy the complete text of article (Russian version a format - PDF) or to read the material which is in open access only the authorized visitors of the website can. .