Determination of reservoir rock residual water using X-ray computed microtomography

UDK: 622.276.031.011.431
DOI: 10.24887/0028-2448-2018-3-38-42
Key words: X-ray tomography, virtual cubes, residual water, integral intensity
Authors: I.V. Yazynina (Gubkin Russian State University of Oil and Gas (National Research University), RF, Moscow), E.V. Shelyago (Gubkin Russian State University of Oil and Gas (National Research University), RF, Moscow), A.A. Abrosimov (Gubkin Russian State University of Oil and Gas (National Research University), RF, Moscow), N.E. Grachev (Lomonosov Moscow State University, RF, Moscow), D.A. Bikulov (Lomonosov Moscow State University, RF, Moscow)

Registration of fluids (oil, water and gas) in reservoir rocks is one of the tasks, that researchers solve using X-ray computed microtomography (MCT). One can find many works in this area in open literature, but most of them use bulk models or coarse rocks as research objects. Such porous systems with pores and channels size of several tens or even hundreds of micrometers allow micron resolution MCT-shooting, which is sufficient for visualization of wetting and non-wetting phases. Due to the resolution lack, finely porous saturated system study is limited, though they make up a large share of oil and gas reservoirs.

Goal of current labor is to assess opportunities and to create new approaches of MCT usage for residual water determination.  There was no task for direct phase visualization because of practical application absence. This decision was contributed by analysis of core samples’ capillary curves - a significant part of filter channels and pores filled with residual water have sub-micron size.

Four methods of residual water estimation were tested: excretion of water absorption spectrum (with radiopaque and without it), analysis of integral intensity absorption spectra, analysis of single-phase flow rates field (completely calculation method). Last two methods are new and they were used for rock study for the first time. Results of residual water estimation by new methods were compared with laboratory measurements. Calculation method of single-phase flow rates field analysis for limited number of core samples allowed to obtain correlations between porosity and residual water, that are close to the actual laboratory trend for entire reservoir.

References

1. Di Michiel Marco, Merino J.M., Fernandez-Carreiras D. et al., Fast microtomography using high energy synchrotron radiation, Review of Scientific Instruments, 2005, V. 76.

2. Porter M.L., Wildenschild D., Grant G., Gerhard J.I., Measurement and prediction of the relationship between capillary pressure, saturation, and interfacial area in a NAPL‐water‐glass bead system, Water resources research, 2010, V. 46.

3. Petrovic A.M., Siebert J.E., Rieke P.E., Soil bulk-density analysis in 3 dimensions by computed tomographic scanning, Soil Sci. Soc. Am. J., 1982, V. 46 (3), pp. 445–450.

4. Withjack E.M., Computed tomography for rock-property determination and fluid-flow visualization, SPE 16951-PA, 1988.

5. Coles M.E. et al., Pore level imaging of fluid transport using synchrotron

X-ray microtomography, J. Petrol. Sci. Eng., 1998, V. 19 (1–2), pp. 55–63,

6. Wildenschild D., J.W. Hopmansc, Vazd C.M.P. et al., Using X-ray computed tomography in hydrology: systems, resolutions, and limitations, Journal of Hydrology, 2002, V. 267, pp. 285–297.

7. Turner M., Three-dimensional imaging of multiphase flow in porous media, Physica A, 2004, V. 339 (1–2), pp. 166–72.

8. Silin D., Tomutsa L., Benson S.M., Padzek T.W., Microtomography and pore-scale modeling of two-phase fluid distribution, Transport in Porous Media, 2011, V. 86, no. 2, pp. 495–515.

9. Al-Raoush R., Willson C., A pore-scale investigation of a multiphase porous media system, J. Contam. Hydrol., 2005. V. 77(1–2), pp. 67–89.

10. Matthew A., Branko B., Martin J., Blunt pore-scale contact angle measurements at reservoir conditions using X-ray microtomography, Advances in Water Resources, 2014, V. 68, pp. 24–31.

11. Dodd N., Marathe R., Middleton J. et al., Pore-scale imaging of oil and wettability in native-state, mixed-wet reservoir carbonates, International Petroleum Technology Conference, 19-22 January, Doha, Qatar, 2014.

12. Kumar M. et al., Imaging of pore scale distribution of fluids and wettability, International symposium of the society of core analysts, SCA2008-16, 2008.

13. Mees F., Swennen R., Geet M. Van, Jacobs P., Applications of X-ray computed tomography in the geosciences, The Geological Society, 2003.

14. Yazynina I.V., Shelyago E.V., Abrosimov A.A., Veremko N.A., Grachev N.E., Senin D.S., Novel approach to core sample MCT research for practical petrophysics problems solution (In Russ.), Neftyanoe khozyaystvo = Oil Industry, 2017, no. 1, pp. 19–23.

15. Yazynina I.V., Shelyago E.V., Abrosimov A.A. et al., Testing a new approach to petrophysical trend determination from X-Ray tomography (In Russ.), Neftyanoe khozyaystvo = Oil Industry, 2017, no. 2, pp. 36–40.



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